Correlation between water uptake and biaxial flexural strength in restorative composites
DOI:
https://doi.org/10.11606/issn.2357-8041.v20i2p67-73Keywords:
Materiais DentáriosAbstract
Though aging of resin composites has been the subject of several investigations, the correlation between strength and water uptake has not been established. Therefore, the purpose of the present study was to verify if there was a statistically significant correlation between biaxial flexural strength and weight gain due to water uptake for two commercial restorative composites, one methacrylate-based and one silorane-based. Discs (15 mm in diameter by 1 mm thick) were built with either Filtek Z250 or Filtek Silorane (both from 3M ESPE) and dry stored for 30 days. Then, they were weighted in an analytical balance and immersed in distilled water at 37 oC for 1, 2, 5, 7, 30 or 60 days (n=10). After the immersion period, the discs were re-weighted and immediately fractured on a “piston-on-three-ball” device. Mass gain (in percentage) and biaxial flexural strength data were subjected to two-way ANOVA/Tukey test and Pearson’s correlation analysis (alpha: 5%). Mass gain was similar for both composites in a given storage period, and did not vary significantly between one and seven days. For Filtek Z250, biaxial strength decreased gradually with prolonged immersion, while for Filtek Silorane, it decreased abruptly between 30 and 60 days. Statistically significant correlations were found between strength and mass gain for both composites. However, a stronger correlation was found for Filtek Z250 (r=-0.706, p<0.001) compared to Filtek Silorane (r= - 0.361, p<0.01). Therefore, it was possible to conclude that strength is linearly related to water uptake and this correlation is material-dependent.Downloads
References
Braden M, Causton EE and Clarke RL. Diffusion of water in composite filling materials. J Dent Res 1976; 55: 730-2.
Thompson LR, Miller EG and Bowles WH. Leaching of unpolymerized materials from orthodontic bonding resin. J Dent Res 1982; 61: 989-92.
Ferracane JL. Elution of leachable components from composites. J Oral Rehabil 1994; 21: 441-52.
Forss H and Widstrom E. Reasons for restorative therapy and the longevity of restorations in adults. Acta Odontol Scand 2004; 62: 82-6.
Demarco FF, Correa MB, Cenci MS, Moraes RR and Opdam NJ. Longevity of posterior composite restorations: not only a matter of materials. Dent Mater 2012; 28: 87-101.
Ferracane JL, Berge HX and Condon JR. In vitro aging of dental composites in water--effect of degree of conversion, filler volume, and filler/matrix coupling. J Biomed Mater Res 1998; 42: 465-72.
Kalachandra S and Wilson TW. Water sorption and mechanical properties of light-cured proprietary composite tooth restorative materials. Biomaterials 1992; 13: 105-9.
Sideridou I, Tserki V and Papanastasiou G. Study of water sorption, solubility and modulus of elasticity of light-cured dimethacrylate-based dental resins. Biomaterials 2003; 24: 655-65.
Yiu CK, King NM, Pashley DH, Suh BI, Carvalho RM, Carrilho MR and Tay FR. Effect of resin hydrophilicity and water storage on resin strength. Biomaterials 2004; 25: 5789-96.
Tarumi H, Torii M and Tsuchitani Y. Relationship between particle size of barium glass filler and water sorption of light-cured composite resin. Dent Mater J 1995; 14: 37-44.
Ilie N and Hickel R. Macro-, micro- and nano-mechanical investigations on silorane and methacrylate-based composites. Dent Mater 2009; 25: 810-9.
Sideridou ID, Karabela MM and Vouvoudi E. Physical properties of current dental nanohybrid and nanofill light-cured resin composites. Dent Mater 2011; 27: 598-607.
Hahnel S, Henrich A, Burgers R, Handel G and Rosentritt M. Investigation of mechanical properties of modern dental composites after artificial aging for one year. Oper Dent 2010; 35: 412-9.
Ito S, Hashimoto M, Wadgaonkar B, Svizero N, Carvalho RM, Yiu C, Rueggeberg FA, Foulger S, Saito T, Nishitani Y, Yoshiyama M, Tay FR and Pashley DH. Effects of resin hydrophilicity on water sorption and changes in modulus of elasticity. Biomaterials 2005; 26: 6449-59.
Musanje L, Shu M and Darvell BW. Water sorption and mechanical behaviour of cosmetic direct restorative materials in artificial saliva. Dent Mater 2001; 17: 394-401.
ISO 4049: Dentistry - Polymer-based filling, restorative and luting materials. 2000;
Pick B, Meira JB, Driemeier L and Braga RR. A critical view on biaxial and short-beam uniaxial flexural strength tests applied to resin composites using Weibull, fractographic and finite element analyses. Dent Mater 2010; 26: 83-90.
ISO 6872: Dentistry - dental ceramics. 1999;
Chung SM, Yap AU, Koh WK, Tsai KT and Lim CT. Measurement of Poisson's ratio of dental composite restorative materials. Biomaterials 2004; 25: 2455-60.
Palin WM, Fleming GJ, Burke FJ, Marquis PM and Randall RC. The influence of short and medium-term water immersion on the hydrolytic stability of novel low-shrink dental composites. Dent Mater 2005; 21: 852-63.
Boaro LC, Goncalves F, Guimaraes TC, Ferracane JL, Pfeifer CS and Braga RR. Sorption, solubility, shrinkage and mechanical properties of "low-shrinkage" commercial resin composites. Dent Mater 2013; 29: 398-404.
Guggenberger R and Weinmann W. Exploring beyond methacrylates. Am J Dent 2000; 13: 82D-84D.
Arrais CA, de Oliveira MT, Mettenburg D, Rueggeberg FA and Giannini M. Silorane- and high filled-based "low-shrinkage" resin composites: shrinkage, flexural strength and modulus. Braz Oral Res 2013; 27: 97-102.
Schneider LF, Cavalcante LM, Silikas N and Watts DC. Degradation resistance of silorane, experimental ormocer and dimethacrylate resin-based dental composites. J Oral Sci 53: 413-9.
Downloads
Published
Issue
Section
License
Authors are requested to send, together with the letter to the Editors, a term of responsibility. Thus, the works submitted for appreciation for publication must be accompanied by a document containing the signature of each of the authors, the model of which is presented as follows:
I/We, _________________________, author(s) of the work entitled_______________, now submitted for the appreciation of Clinical and Laboratorial Research in Dentistry, agree that the authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal. Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgement of its initial publication in this journal. Authors are permitted and encouraged to post their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work (See The Effect of Open Access).
Date: ____/____/____Signature(s): _______________